Comparison of analytical techniques for the determination of organophosphate pesticides in agricultural samples

Authors

DOI:

https://doi.org/10.33064/iycuaa2022853168

Keywords:

Pesticides, environmental, analytical method, residue, chromatography, spectrophometry

Abstract

Pesticides are considered substances of interest and target of study due to the secondary effects they have on the environment and on human health. The monitoring of pesticide residues is important to trace the possible contamination of the food we consume daily. The objective was to compare two techniques for the validation of spectrophotometry as a detection alternative. Soil, water and chili samples from the states of Aguascalientes, Sinaloa and Tamaulipas were evaluated by high efficiency liquid chromatography and spectrophotometry. The data was compared with the R 3.6 program and the 1.3 agricolae package. Statistical similarity was observed in the monitored pesticides: Malathion, methamidophos and chlorpyrifos, for which, spectrophotometry is recommended as an alternative detection technique for these, however, for monocrotophos  further studies are suggested.

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Author Biographies

Valeria Maldonado-Ortega, Universidad Autónoma Agraria Antonio Narro

Departamento de Parasitología

Ernesto Cerna-Chávez, Universidad Autónoma Agraria Antonio Narro

Doctor en Ciencias en Parasitología Agrícola, Profesor Investigador Universidad Autónoma Agraria Antonio Narro, Departamento de Parasitología Agrícola

Yisa María Ochoa-Fuentes, Universidad Autónoma Agraria Antonio Narro

Doctora en Ciencias en Parasitología Agrícola, Profesora Investigadora Universidad Autónoma Agraria Antonio Narro, Departamento de Parasitología Agrícola.

References

• Araoud, M., Douki, W., Rhim, A., Najjar, M.F., y Gazzah, N. (2007). Multiresidue analysis of pesticides in fruits and vegetables by gas chromatography-mass spectrometry. Journal of Environmental Science and Health, 42, 179–187. DOI: 10.1080/03601230601123474.

• Hird, S.J., Lau, B.P.Y., Schuhmacher R., y Krska, R. (2014). Liquid chromatography-mass spectrometry for the determination of chemical contaminants in food. Trends in Analytical Chemistry, 59, 59-72. DOI: 10.1016/j.trac.2014.04.005

• Maldonado, V., Ochoa, Y. M., y Cerna, E. (2020). Determinación de plaguicidas organofosforados a trabajadores de control de plagas del estado de Coahuila. Horizonte Sanitario, 19 (2), 217-222. https://doi.org/10.19136/hs.a19n2.3640

• Romero A., Palchetti, I., Avelar M., González E., Garate J.L., & Torres E. (2019). Spectrophotometric detection of glyphosate in water by complex formation between Bis 5-phenyldipyrrinate of Nickel (II) and glyphosate. Water, 11, 719. DOI: 10.3390/w11040719

• Yanjie Li., Changjun H., Jincan L., Bo D., Jing H., & Mei Y. (2016). Detection of organophosphorus pesticides with colorimetry and computer image analysis. Analytical Sciences, 32, 719-724. DOI: 10.2116/analsci.32.719

Published

2022-04-30

How to Cite

Maldonado-Ortega, V., Cerna-Chávez, E., Hernández-Bautista, O., & Ochoa-Fuentes, Y. M. (2022). Comparison of analytical techniques for the determination of organophosphate pesticides in agricultural samples. Investigación Y Ciencia De La Universidad Autónoma De Aguascalientes, (85). https://doi.org/10.33064/iycuaa2022853168

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